How to plan for dirty samples for both extraction and analysis

When juggling the responsibilities of working in a sample preparation lab as well as working as an analyst, it is very easy to get caught up in a never-ending cycle of samples. There is no situation “more frustrating” then when you have a bunch of wastewater samples that need to be extracted and analyzed ASAP and there is that one sample that is so much more challenging to extract than the others. After struggling all-day-long, you finally get the batch of rush samples set up to run on your gas chromatography (GC) system overnight only to come in the next morning to find that your mid and closing check standards are low and the data is effectively useless!

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The Secret to Tackling Dirty Samples – Tips & Tricks for Filtering

Solid phase extraction is a powerful technique – it can be used to clean up the most challenging samples, and extract and preconcentrate hundreds of semivolatile organic compounds.  When performing the extraction, the goal is to get the entire sample to run through the extraction disk.  But in order to do that, the disk must have the chemical and physical capacity to handle your sample matrix.  If your disk becomes overwhelmed or clogs, you risk losing your sample and the chance to complete your extraction.

How do you prevent the disk from clogging?  Prefilters!

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